Methanesulfonyl chloride → HCID 86676750, compound

HRID 2411128Notes

Reaction equation

HRID 2411128 reaction equation
[NH2:1][C@H:2]([CH2:5][CH3:6])[CH2:3]O.[CH3:7][S:8](Cl)(=[O:10])=[O:9]>>[CH2:5]([C@@H:2]1[CH2:3][CH2:7][S:8](=[O:10])(=[O:9])[NH:1]1)[CH3:6]

Participants

3

Reactant 2

HCID 31297Methanesulfonyl chlorideHCID 27238562-Amino-1-butanol, (-)-

Product 1

HCID 86676750HCID 86676750, compound

Procedure

Using (R)-2-amino-1-butanol (1.78 g) and methanesulfonyl chloride (3.2 mL) and by the reaction and treatment in the same manner as in Preparation Example 1, the title compound (1.54 g) was obtained.

Workup

  1. customby the reaction and treatment in the same manner
  2. customas in Preparation Example 1

Sources & evidence

ORD record
ord-6446008fab1744269fe765a108510a88
Source dataset
uspto-grants-2014_08
Patent number
US08816079B2

Reaction notes

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