Methanesulfonyl chloride → HCID 86676752, compound

HRID 2411130Notes

Reaction equation

HRID 2411130 reaction equation
[NH2:1][C@@H:2]([CH:5]([CH3:7])[CH3:6])[CH2:3]O.[CH3:8][S:9](Cl)(=[O:11])=[O:10]>>[CH:5]([C@H:2]1[CH2:3][CH2:8][S:9](=[O:11])(=[O:10])[NH:1]1)([CH3:7])[CH3:6]

Participants

3

Reactant 2

HCID 31297Methanesulfonyl chlorideHCID 640993L-Valinol

Product 1

HCID 86676752HCID 86676752, compound

Procedure

Using (S)-2-amino-3-methyl-1-butanol (5.0 g) and methanesulfonyl chloride (7.7 mL) and by the reaction and treatment in the same manner as in Preparation Example 1, the title compound (1.55 g) was obtained.

Workup

  1. customby the reaction and treatment in the same manner
  2. customas in Preparation Example 1

Sources & evidence

ORD record
ord-5cd9e7102c4b4cc1807ada16024c156c
Source dataset
uspto-grants-2014_08
Patent number
US08816079B2

Reaction notes

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