huagongshe.com
HRID2411135

反应详情

EQUATION

反应方程式

HRID 2411135 的结构方程式

REACTANTS

反应物

2
结构：O=S1(=O)CC[C@@H](COCc2ccccc2)N1
HCID16664117

未命名化合物

结构：COC(=O)c1ccc(Br)cc1N1CCCS1(=O)=O
HCID58484624

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)c1ccc(N2[C@H](COCc3ccccc3)CCS2(=O)=O)cc1N1CCCS1(=O)=O
HCID71261161

未命名化合物

收率 87.1%

PROCEDURE

实验过程

Using methyl 4-bromo-2-(1,1-dioxo-1λ6-isothiazolidin-2-yl)benzoate (334 mg) described in Preparation Example 13 and (S)-3-benzyloxymethylisothiazolidine 1,1-dioxide (241 mg) described in Preparation Example 1 and by the reaction and treatment in the same manner as in Preparation Example 12, the title compound (430 mg) was obtained.

WORKUP

后处理

  1. customdescribed in Preparation Example 1 and by the reaction and treatment in the same manner as in Preparation Example 12