Dichloromethane → HCID 71252328, compound

Participants

Reaction Steps

To a mixture of p-(methoxycarbonyl)phenylboronic acid (2.45 g), 1-acetylimidazolidin-2-one (870 mg) and copper(II) acetate (1.23 g) were added methylene chloride (20 mL) and triethylamine (1.9 mL), and the mixture was stirred at room temperature overnight. Water was added to the reaction mixture, and the insoluble material was collected by filtration. The filtrate was extracted with chloroform, and the solvent was evaporated from the organic layer. The obtained residue was purified by column chromatography (chloroform) to give the title compound (292 mg).

Provenance & Evidence