HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromobenzoyl chloride → (4-Bromophenyl)[4-(2,4-dimethylphenyl)piperazin-1-yl]methanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromobenzoyl chloride | HCID 68515 | — |
| Reactant | 1-(2,4-Xylyl)piperazine | HCID 70544 | — |
| Product | (4-Bromophenyl)[4-(2,4-dimethylphenyl)piperazin-1-yl]methanone | HCID 58484623 | 72.9% |
Reaction Steps
Using 4-bromobenzoyl chloride (25 g) and 1-(2,4-dimethylphenyl)piperazine (22 g) and by the reaction and treatment in the same manner as in Preparation Example 108, the title compound (31 g) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-c83b198c976a425595a535bf355a1454 |
| Source note | uspto-grants-2014_08 |