HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2,4-Xylyl)piperazine → HCID 71251979, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2,4-Xylyl)piperazine | HCID 70544 | — |
| Reactant | 4-Bromo-2-cyanobenzoic acid | HCID 58484585 | — |
| Product | HCID 71251979 | HCID 71251979 | 84% |
Reaction Steps
Using 4-bromo-2-cyanobenzoic acid (1.81 g) described in Preparation Example 76 and 1-(2,4-dimethylphenyl)piperazine (1.67 g) and by the reaction and treatment in the same manner as in Preparation Example 111, the title compound (2.68 g) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-334e8fdfb2904a828fe609cd0c11e370 |
| Source note | uspto-grants-2014_08 |