4-Methyloxybenzyl chloride → HCID 71252043, compound

HRID 2411341Notes

Reaction equation

HRID 2411341 reaction equation
[CH2:1]([CH:3]1[NH:7][C:6](=[O:8])[NH:5][C:4]1=[O:9])[CH3:2].[CH3:10][O:11][C:12]1[CH:19]=[CH:18][C:15]([CH2:16]Cl)=[CH:14][CH:13]=1>>[CH2:1]([CH:3]1[NH:7][C:6](=[O:8])[N:5]([CH2:16][C:15]2[CH:18]=[CH:19][C:12]([O:11][CH3:10])=[CH:13][CH:14]=2)[C:4]1=[O:9])[CH3:2]

Participants

3

Reactant 2

HCID 699934-Methyloxybenzyl chlorideHCID 2532172-Ethylhydantoin

Product 1

HCID 71252043HCID 71252043, compound

Procedure

Using 5-ethylimidazolidine-2,4-dione (2.00 g) and 4-methoxybenzyl chloride (2.54 mL) and by the reaction and treatment in the same manner as in Preparation Example 51, the title compound (3.08 g) was obtained.

Workup

  1. customby the reaction and treatment in the same manner
  2. customas in Preparation Example 51

Sources & evidence

ORD record
ord-8964eb341b0942259eae5b4939da2e48
Source dataset
uspto-grants-2014_08
Patent number
US08816079B2

Reaction notes

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