Methyl iodide → 3,5-Dimethyl-2,4-Imidazolidinedione

HRID 2411348Notes

Reaction equation

HRID 2411348 reaction equation
[CH3:1][CH:2]1[NH:6][C:5](=[O:7])[NH:4][C:3]1=[O:8].[CH3:9]I>>[CH3:9][N:4]1[C:3](=[O:8])[CH:2]([CH3:1])[NH:6][C:5]1=[O:7]

Participants

3

Reactant 2

HCID 6328Methyl iodideHCID 692165-Methylhydantoin

Product 1

HCID 101540613,5-Dimethyl-2,4-Imidazolidinedione

Procedure

Using 5-methylimidazolidine-2,4-dione (1.00 g) and methyl iodide (0.57 mL) and by the reaction and treatment in the same manner as in Preparation Example 214, the title compound (1.66 g, containing DMF) was obtained.

Workup

  1. customby the reaction and treatment in the same manner
  2. customas in Preparation Example 214

Sources & evidence

ORD record
ord-6a391b4510b048bf8b2cb1df12641ef4
Source dataset
uspto-grants-2014_08
Patent number
US08816079B2

Reaction notes

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