HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3,5-Dimethylpyridin-2-yl)piperazine → HCID 86676765, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3,5-Dimethylpyridin-2-yl)piperazine | HCID 58484496 | — |
| Reactant | 6-Bromo-4-methyl-3-pyridinecarboxylic acid | HCID 72212158 | — |
| Product | HCID 86676765 | HCID 86676765 | 97.7% |
Reaction Steps
Using 6-bromo-4-methylnicotinic acid (500 mg) and 1-(3,5-dimethylpyridin-2-yl)piperazine (443 mg) described in Preparation Example 79 and by the reaction and treatment in the same manner as in Preparation Example 111, the title compound (880 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-e09ec244a812476aa832513335e741b7 |
| Source note | uspto-grants-2014_08 |