HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2-methoxybenzoic acid → HCID 71252877, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2-methoxybenzoic acid | HCID 13450755 | — |
| Reactant | 1-(3,5-Dimethylpyridin-2-yl)piperazine | HCID 58484496 | — |
| Product | HCID 71252877 | HCID 71252877 | 94.4% |
Reaction Steps
Using 4-bromo-2-methoxybenzoic acid (2.31 g) and 1-(3,5-dimethylpyridin-2-yl)piperazine (1.91 g) described in Preparation Example 79 and by the reaction and treatment in the same manner as in Preparation Example 111, the title compound (3.81 g) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-da47bcf746454e6b8be32e42f2a99cbb |
| Source note | uspto-grants-2014_08 |