HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Butanesultam → HCID 71251881, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Butanesultam | HCID 303508 | — |
| Reactant | (6-Bromopyridin-3-yl)[4-(3,5-dimethylpyridin-2-yl)piperazin-1-yl]methanone | HCID 58484661 | — |
| Product | HCID 71251881 | HCID 71251881 | 73% |
Reaction Steps
Using (6-bromopyridin-3-yl)[4-(3,5-dimethylpyridin-2-yl)piperazin-1-yl]methanone (188 mg) described in Preparation Example 127 and [1,2]thiazinane 1,1-dioxide (68 mg) and by the reaction and treatment in the same manner as in Example 1, the title compound (157 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-1c3d855d264c4e09aeea7477ffffbbb5 |
| Source note | uspto-grants-2014_08 |