HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Methyl-2-pyrrolidone → HCID 71252761, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Methyl-2-pyrrolidone | HCID 66055 | — |
| Reactant | (4-Bromo-2-methanesulfonylphenyl)[4-(3,5-dimethylpyridin-2-yl)piperazin-1-yl]methanone | HCID 58484505 | — |
| Product | HCID 71252761 | HCID 71252761 | 33.8% |
Reaction Steps
Using (4-bromo-2-methanesulfonylphenyl)[4-(3,5-dimethylpyridin-2-yl)piperazin-1-yl]methanone (864 mg) described in Preparation Example 112 and 5-methylpyrrolidin-2-one (258 mg) and by the reaction and treatment in the same manner as in Example 1, the title compound (304 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-067bd09226e741c48948bb68ff95f99b |
| Source note | uspto-grants-2014_08 |