HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Butanesultam → HCID 71252223, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Butanesultam | HCID 303508 | — |
| Reactant | HCID 71252294 | HCID 71252294 | — |
| Product | HCID 71252223 | HCID 71252223 | 86.7% |
Reaction Steps
Using 5-bromo-2-[4-(3,5-dicyclopropylpyridin-2-yl)piperazine-1-carbonyl]benzonitrile (451 mg) described in Preparation Example 245 and [1,2]thiazinane 1,1-dioxide (176 mg) and by the reaction and treatment in the same manner as in Example 262, the title compound (438 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-a16f83d0f1e44b0db8313a224c9c3cf6 |
| Source note | uspto-grants-2014_08 |