HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Propanesultam → HCID 71252368, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Propanesultam | HCID 642157 | — |
| Reactant | HCID 71252298 | HCID 71252298 | — |
| Product | HCID 71252368 | HCID 71252368 | 92.6% |
Reaction Steps
Using 5-bromo-2-[4-(5-ethyl-3-methylpyridin-2-yl)piperazine-1-carbonyl]benzonitrile (1.24 g) described in Preparation Example 246 and isothiazolidine 1,1-dioxide (0.47 g) and by the reaction and treatment in the same manner as in Example 262, the title compound (1.26 g) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-f3c61cc3ebba4383a0b51359e446f084 |
| Source note | uspto-grants-2014_08 |