HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 71251970, compound → HCID 71252347, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 71251970 | HCID 71251970 | — |
| Solvent | Dimethylamine tetrahydrofuran | HCID 22320367 | — |
| Product | HCID 71252347 | HCID 71252347 | 43.3% |
Reaction Steps
Using N,N-di-tert-butyloxycarbonyl-5-(1,1-dioxo-1λ6-isothiazolidin-2-yl)-2-[4-(3,5,6-trimethylpyridin-2-yl)piperazine-1-carbonyl]benzamide (202 mg) described in Example 768 and 2 mol/L dimethylamine tetrahydrofuran solution (180 μL) and by the reaction and treatment in the same manner as in Example 770, the title compound (65 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-bc62bb35b59f475fa398ae3a4d9dd1a2 |
| Source note | uspto-grants-2014_08 |