HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 71252354, compound → HCID 71252300, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 71252354 | HCID 71252354 | — |
| Solvent | Dimethylamine tetrahydrofuran | HCID 22320367 | — |
| Product | HCID 71252300 | HCID 71252300 | 50.9% |
Reaction Steps
Using N,N-di-tert-butyloxycarbonyl-2-[4-(3,5-dimethylpyridin-2-yl)piperazine-1-carbonyl]-5-(2-methyl-5-oxopyrrolidin-1-yl)benzamide (70 mg) described in Example 837 and 2 mol/L dimethylamine tetrahydrofuran solution (220 μL) and by the reaction and treatment in the same manner as in Example 770, the title compound (26 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-45ffe021850e40b19b45a30e30c559bd |
| Source note | uspto-grants-2014_08 |