HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 54398791, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 54455625 | HCID 54455625 | — |
| Product | HCID 54398791 | HCID 54398791 | — |
Reaction Steps
The azlactone from Example 67 was suspended in acetone and heated for 10 minutes on a steam bath. Addition of 2N HCl and extractive work-up gave 4-(2-benzoylamino-2-carboxyvinyl)-2-fluoro-1-triphenylmethylimidazole, having the following n.m.r. in CDCl3 : 6.88 (s, 1H); 6.95-7.7 (m, 19H); 8.1-8.3 (m, 2H); 13.09 (br s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04492692 |
| Source dataset | uspto-grants-1985_01 |
| ORD ID | ord-6775535f27a24d06bc554f5f8025f417 |
| Source note | uspto-grants-1985_01 |