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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2412804Generated: October 31, 2026

HCID 23315738, compound → HCID 23315735, compound

https://huagongshe.com/reaction/2412804

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 23315738HCID 23315738—
ReactantPhthalimide potassium saltHCID 24194345—
SolventDimethylformamideHCID 6228—
ProductHCID 23315735HCID 2331573583.1%

Reaction Conditions

Temperature60 °C

Reaction Steps

A mixture of N-(4-chloromethylbenzyloxy)phthalimide (18.5 g.) and potassium phthalimide (15.4 g.) in N,N-dimethylformamide (180 ml.) was stirred at 60° C. for 5 hours. The mixture was poured into ice-water and the precipitates were collected by filtration. The precipitate were washed with water and acetone in turn to give N-(4-phthalimidomethylbenzyloxy)phthalimide (21.0 g.).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04493833
Source datasetuspto-grants-1985_01
ORD IDord-b6870b330d70494c9ff6c6583948fdc3
Source noteuspto-grants-1985_01