Acetyl chloride → HCID 20432112, compound

Participants

Reaction Steps

In like manner as in Preparation Example 1, 200 g of this 1-phenyl-1-(4'-tert-butylphenyl)ethane was reacted with acetyl chloride to obtain 1-(4-acetylphenyl)-1-(4'-tert-butylphenyl)ethane. Also in like manner as in Preparation Example 1, this compound was converted into an alcohol by using sodium borohydride, and the product was then dehydrated with potassium hydrogensulfate to obtain 1-(4-tert-butylphenyl)-1-(4'-vinylphenyl)ethane in a yield of 69.2% (b.p. 171° C./10 mmHg, 130° C./2 mmHg).

Provenance & Evidence