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HRID 2412822생성일: 2026년 10월 25일

Hydrochloric Acid → Methane

https://huagongshe.com/reaction/2412822

반응식

참여 물질

역할이름HCID투입량
반응물Hydrochloric AcidHCID 313—
반응물EthanolHCID 702—
반응물4-(Dimethylamino)BenzaldehydeHCID 7479—
반응물1H-Indole, 1-ethyl-2-methyl-HCID 170432—
반응물Sodium p-toluenesulfinateHCID 2723791—
생성물MethaneHCID 297—
생성물[(4-Dimethylaminophenyl)(1-ethyl-2-methyl-3-indolyl)(4-methylphenylsulfonyl)]methaneHCID 20184815—

반응 단계

Proceeding in a manner similar to that described in Example 1 above substituting for ethyl alcohol and the concentrated hydrochloric acid the appropriate reaction medium and the appropriate catalyst listed in Examples 58-82 of Table A hereinbelow, 4-dimethylaminobenzaldehyde, sodium p-toluenesulfinate and 1-ethyl-2-methylindole were interacted at the indicated temperature to obtain a methane of Formula II wherein R=4--CH3 ; R1 =CH3 ; R3 =R5 =H; R6 =N(CH3)2. A toluene or acetone solution of the product from Examples 58-82 contacted with silica gel developed at blue-red colored image.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04494989
출처 데이터셋uspto-grants-1985_01
ORD IDord-9844834c967443a9a82115fbb841dac2
출처 메모uspto-grants-1985_01