Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → Methane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | 4-(Dimethylamino)Benzaldehyde | HCID 7479 | — |
| 반응물 | 1H-Indole, 1-ethyl-2-methyl- | HCID 170432 | — |
| 반응물 | Sodium p-toluenesulfinate | HCID 2723791 | — |
| 생성물 | Methane | HCID 297 | — |
| 생성물 | [(4-Dimethylaminophenyl)(1-ethyl-2-methyl-3-indolyl)(4-methylphenylsulfonyl)]methane | HCID 20184815 | — |
반응 단계
Proceeding in a manner similar to that described in Example 1 above substituting for ethyl alcohol and the concentrated hydrochloric acid the appropriate reaction medium and the appropriate catalyst listed in Examples 58-82 of Table A hereinbelow, 4-dimethylaminobenzaldehyde, sodium p-toluenesulfinate and 1-ethyl-2-methylindole were interacted at the indicated temperature to obtain a methane of Formula II wherein R=4--CH3 ; R1 =CH3 ; R3 =R5 =H; R6 =N(CH3)2. A toluene or acetone solution of the product from Examples 58-82 contacted with silica gel developed at blue-red colored image.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04494989 |
| 출처 데이터셋 | uspto-grants-1985_01 |
| ORD ID | ord-9844834c967443a9a82115fbb841dac2 |
| 출처 메모 | uspto-grants-1985_01 |