反应详情

2-Nitrobenzylchloride dissolved in ethanol is heated at reflux with a 10% molar excess of sodium azide for from six to eight hours. Insoluble salts are removed by filtration, the ethanol removed, and the resultant oil is dissolved in diethyl ether. Additional insoluble material is removed by filtration and 2-nitrobenzylazide is obtained as a pale yellow oil by removal of the diethyl ether.

1. temperatureis heated
2. customInsoluble salts are removed by filtration
3. customthe ethanol removed
4. dissolutionthe resultant oil is dissolved in diethyl ether
5. customAdditional insoluble material is removed by filtration