HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 15919396, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Methacryloyl chloride | HCID 13528 | — |
| Reactant | N-(4-Amino-2-hydroxyphenyl)-2,2,3,3,4,4,4-heptafluorobutyramide | HCID 70060 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 15919396 | HCID 15919396 | 61.8% |
Reaction Steps
To 64 g (0.2 mol) of 2-heptafluorobutanamido-5-aminophenol were added 18 g (0.22 mol) of pyridine and 500 ml of acetonitrile and mixture was cooled with stirring. To the solution was added dropwise 23 g (0.22 mol) of methacrylic chloride. After the completion of the reaction, 500 ml of water was added to the reaction solution and the crystals thus deposited were collected and recrystallized from acetonitrile to obtain 48 g of Monomer Coupler (15).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04495272 |
| Source dataset | uspto-grants-1985_01 |
| ORD ID | ord-05698099a82b4ae3b17db3a42444e607 |
| Source note | uspto-grants-1985_01 |