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Hydrazine hydrate (1:1) → 5-METHOXY-alpha,alpha-DIMETHYL-1H-INDOL-3-YL-ETHANEAMINE
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrazine hydrate (1:1) | HCID 24654 | — |
| 反応物 | 5-methoxy-3-(2,2-dimethyl-2-nitroethyl)-1H-indole | HCID 12619662 | — |
| 触媒 | Nickel | HCID 935 | — |
| 生成物 | 5-METHOXY-alpha,alpha-DIMETHYL-1H-INDOL-3-YL-ETHANEAMINE | HCID 12619664 | — |
反応手順
The nitro compound produced in Procedure 11C was reduced with Raney nickel and hydrazine hydrate according to the method of Procedure 10D. The structure of the product was confirmed by examination of the NMR spectrum, m.p. 114°-116°, yield 25.8 g. from 31.3 g. of nitro compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04495352 |
| 出典データセット | uspto-grants-1985_01 |
| ORD ID | ord-9f8dce3276804b1696562589c2439a5e |
| 出典メモ | uspto-grants-1985_01 |