HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → 2,2-Dimethyl-1,3-dioxane-4,6-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Malonic Acid | HCID 867 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Product | 2,2-Dimethyl-1,3-dioxane-4,6-dione | HCID 16249 | — |
Reaction Steps
As described in CA 2:14217, 52 g. of malonic acid, 60 ml. of acetic anhydride, 1.5 ml. of sulfuric acid and 40 ml. of acetone were stirred at 0° for 8 hours. The solid was filtered and washed with water, giving 37 g. of product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04496368 |
| Source dataset | uspto-grants-1985_01 |
| ORD ID | ord-ebb317cb88ef4a8aa79bb0696bdec070 |
| Source note | uspto-grants-1985_01 |