HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethylamine → 4,6-Dimethoxy-N,N,N-trimethyl-1,3,5-triazin-2-aminium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethylamine | HCID 1146 | — |
| Reactant | 2-Chloro-4,6-dimethoxy-1,3,5-triazine | HCID 18450 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 4,6-Dimethoxy-N,N,N-trimethyl-1,3,5-triazin-2-aminium chloride | HCID 13141331 | — |
Reaction Steps
A solution of 25.0 g of the product from Example 1 in 340 ml dry acetone and 140 ml dry tetrahydrofuran was treated at 0° C. with 21.5 ml of liquid trimethylamine, added over a period of 10 minutes. The resulting thick white reaction mixture was stirred at room temperature for 3 hours. Filtration under nitrogen and drying in vacuo gave 30.4 g of trimethyl(4,6-dimethoxy-1,3,5-triazin-2-yl)ammonium chloride as a white powder, m.p. 130°-134° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04496392 |
| Source dataset | uspto-grants-1985_01 |
| ORD ID | ord-6ed5caf069ef4357bf895dd487a5030d |
| Source note | uspto-grants-1985_01 |