HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl orthoformate → HCID 20429911, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl orthoformate | HCID 31214 | — |
| Reactant | 1-(4-benzoylphenyl)ethanone | HCID 11816948 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20429911 | HCID 20429911 | — |
Reaction Steps
78 g of 4-acetyl-benzophenone is boiled together with 500 ml of ethanol and 200 ml of triethyl orthoformate for 5 hours. The solvent is then distilled off under reduced pressure and the residue is subjected to fractional distillation. 4-(Diethoxyacetyl)-benzophenone is obtained; b.p. 200°/67 P.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04496447 |
| Source dataset | uspto-grants-1985_01 |
| ORD ID | ord-c4576731ea3b4bafa4126d639c17c171 |
| Source note | uspto-grants-1985_01 |