HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl isothiocyanate → HCID 54522826, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl isothiocyanate | HCID 10966 | — |
| Reactant | HCID 20184634 | HCID 20184634 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 54522826 | HCID 54522826 | 70.8% |
Reaction Steps
A mixture of 4-(2-aminopyrid-6-ylthio)butyramide (0.25 g.), ethylisothiocyanate (0.2 g.) and acetonitrile (5 ml.) was heated under reflux for 18 hours and then cooled, and the solid which crystallised was collected to give 4-[2-(3-ethylthioureido)pyrid-6-ylthio]butyramide (0.25 g.) which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04496564 |
| Source dataset | uspto-grants-1985_01 |
| ORD ID | ord-75a513f3f00a44d18123c302b946fd7b |
| Source note | uspto-grants-1985_01 |