HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-(6-methylpyridin-3-yl)prop-2-enoate → Ethyl 3-(6-methyl-3-pyridyl)propionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-(6-methylpyridin-3-yl)prop-2-enoate | HCID 54365744 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethyl 3-(6-methyl-3-pyridyl)propionate | HCID 3018102 | — |
Reaction Steps
Ethyl 3-(6-methyl-3-pyridyl)acrylate (60.36 g) was hydrogenated in ethanol at 35° and 344 kPa using palladium-on-charcoal catalyst (10%, 1.0 g). The mixture was filtered and the filtrate was evaporated to give ethyl 3-(6-methyl-3-pyridyl)propionate as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04496567 |
| Source dataset | uspto-grants-1985_01 |
| ORD ID | ord-c56a99eb65af4c6bbc9bdb99e53e2ce7 |
| Source note | uspto-grants-1985_01 |