HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → 4-Bromo-N,N-dimethylbenzylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | 4-Bromobenzyl bromide | HCID 68527 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 4-Bromo-N,N-dimethylbenzylamine | HCID 235757 | — |
Reaction Steps
Reaction of dimethylamine with 4-bromobenzyl bromide in cold benzene gave 4-bromo-N,N-dimethylbenzylamine which was successively reacted with magnesium, formaldehyde, and cysteamine (in a similar procedure to Example 7) to give 2-[4-(dimethylaminomethyl)benzylthio]ethylamine as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04496567 |
| Source dataset | uspto-grants-1985_01 |
| ORD ID | ord-6b0147df7ddf4a468574272b253534d6 |
| Source note | uspto-grants-1985_01 |