HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propyl Isothiocyanate → HCID 53767345, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propyl Isothiocyanate | HCID 69403 | — |
| Reactant | HCID 20208711 | HCID 20208711 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 53767345 | HCID 53767345 | 64.1% |
Reaction Steps
A mixture of 4-amino-2-(5-phthalimidopentyl)pyrimidine (2 g.) and propylisothiocyanate (1 g.) in pyridine (5 ml.) was heated under reflux for 16 hours then evaporated to dryness. The residual solid was triturated with acetonitrile to give 4-(3-propylthioureido)-2-(5-phthalimidopentyl)pyrimidine (1.7 g.), m.p. 146°-149°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04496571 |
| Source dataset | uspto-grants-1985_01 |
| ORD ID | ord-91405efcc90b458fa441b536b3346538 |
| Source note | uspto-grants-1985_01 |