HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methyl-4-methoxyaniline → HCID 13371479, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methyl-4-methoxyaniline | HCID 7610 | — |
| Reactant | 2-Chlorobenzoic Acid | HCID 8374 | — |
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 13424434 | HCID 13424434 | — |
| Product | HCID 13371479 | HCID 13371479 | — |
Reaction Steps
2-(4-Hydroxy-2-methylphenylamino)benzoic acid [XI; R=H, R"=2-CH3, OH at 4-position], m.p. 209°-211° C. (decompn.) was prepared by boron tribromide demethylation of 2-(4-methoxy-2-methylphenylamino)benzoic acid, in turn prepared by reaction of 2-chlorobenzoic acid with 2-methyl-4-methoxyaniline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04496590 |
| Source dataset | uspto-grants-1985_01 |
| ORD ID | ord-c0d01da9e948430d85b60d5052b16dea |
| Source note | uspto-grants-1985_01 |