HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl p-toluenesulfonate → HCID 86739885, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl p-toluenesulfonate | HCID 6645 | — |
| Reactant | HCID 14548455 | HCID 14548455 | — |
| Product | HCID 86739885 | HCID 86739885 | — |
Reaction Steps
This compound was prepared by quaternization of bis(p-carbomethoxyphenyl)phenylphosphine (I) with methyl p-toluenesulfonate (II) in the melt phase. A mixture of 18.92 g (0.05 mol) of I and 9.31 g (0.05 mol) of II was heated in a 130°-C. bath for 1 hr with stirring. The viscous material was cooled to an amorphous glass which was hygroscopic.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04496643 |
| Source dataset | uspto-grants-1985_01 |
| ORD ID | ord-e9a3a07177e94a0a9380512ea1d7a3d5 |
| Source note | uspto-grants-1985_01 |