Water → HCID 131714190, compound

HRID 2413464Notes

Reaction equation

HRID 2413464 reaction equation
Cl[Si:2](Cl)(Cl)[CH2:3][CH2:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][N:6]=1.O>CO>[SiH3:2][CH2:3][CH2:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][N:6]=1

Participants

4

Reactant 2

HCID 962WaterHCID 869362-[2-(Trichlorosilyl)ethyl]pyridine2×

Product 1

HCID 131714190HCID 131714190, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent2×

Procedure

A solution of 2-(2-silylethyl)pyridine oligosilsesquioxane pillar material was prepared from a methanol solution of 2-(2-trichlorosilylethyl)pyridine (24 grams of 2-(2-trichlorosilylethyl)pyridine in 175 ml of methanol by adding 10.5 ml of water. The mixture was stirred for 1 hour while maintaining the temperature below 30° C.

Workup

  1. temperaturewhile maintaining the temperature below 30° C.

Sources & evidence

ORD record
ord-b4cfba36d9ea4d0d897c1276927d49db
Source dataset
uspto-grants-1988_01
Patent number
US04717513

Reaction notes

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