反应详情

The amide prepared under (a) is dissolved in 50 ml of dry diethyl ether and added dropwise to a suspension of 1.0 g of lithium aluminum hydride in 100 ml of dry diethyl ether. The mixture is then heated under reflux for 3 hours, 5 ml of water is added cautiously to cause decomposition, with cooling, and inorganic material is filtered off. The oil remaining after removal of the solvent in vacuo is reac-ted further without purification.

1. temperatureThe mixture is then heated
2. temperatureunder reflux for 3 hours
3. temperaturewith cooling
4. filtrationinorganic material is filtered off
5. customafter removal of the solvent in vacuo
6. customis reac-ted further without purification