Butylamine → HCID 70411312, compound

HRID 2413528Notes

Reaction equation

HRID 2413528 reaction equation
[S:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[S:10][CH2:11][CH:12]1[C:17](=[O:18])[O:16][C:14](=[O:15])[CH2:13]1.[CH2:19]([NH2:23])[CH2:20][CH2:21][CH3:22].C([NH3+])CCC>>[CH2:19]([NH:23][C:17]([CH:12]([CH2:13][C:14]([OH:16])=[O:15])[CH2:11][S:10][C:2]1[S:1][C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=1)=[O:18])[CH2:20][CH2:21][CH3:22]

Participants

4

Reactant 3

HCID 8007ButylamineHCID 3614750ButylammoniumHCID 539711813-(Benzothiazol-2-ylthio)propane-1,2-dicarboxylic anhydride

Product 1

HCID 70411312HCID 70411312, compound

Procedure

A mixture of 7 parts of 3-(benzothiazol-2-ylthio)-propane-1,2-dicarboxylic anhydride and 3.6 parts of n-butylamine is heated at 55° for 3 hours to give the butylammonium salt of the above amide as a viscous oil (mixture of isomers).

Workup

  1. temperatureis heated at 55° for 3 hours
  2. customto give

Sources & evidence

ORD record
ord-ce549c9b00f548b9801b514eb6ff4e11
Source dataset
uspto-grants-1988_01
Patent number
US04719036

Reaction notes

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