Water → HCID 178443646, compound

HRID 2413529Notes

Reaction equation

HRID 2413529 reaction equation
[S:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[S:10][CH2:11][CH:12]1[C:17](=[O:18])[O:16]C(=O)[CH2:13]1.[CH2:19]([NH2:27])[CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26].[C:28]1(C)C=CC=CC=1.[OH2:35]>>[CH2:19]([N:27]=[C:28]([CH:11]([S:10][C:2]1[S:1][C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=1)[CH:12]([C:17]([OH:16])=[O:18])[CH3:13])[OH:35])[CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26]

Participants

5

Reactant 4

HCID 962WaterHCID 1140TolueneHCID 8143OctylamineHCID 539711813-(Benzothiazol-2-ylthio)propane-1,2-dicarboxylic anhydride

Product 1

HCID 178443646HCID 178443646, compound

Procedure

A solution of 7 parts of 3-(benzothiazol-2-ylthio)-propane-1,2-dicarboxylic anhydride and 3.2 parts of n-octylamine in 100 parts of toluene is heated at 112° for 5 hours until no more water is evolved. Evaporation of the solution gives N-octyl(benzothiazol-2-ylthio)-propane-1,2-dicarboxylic acid imide as a brown oil.

Workup

  1. customEvaporation of the solution

Sources & evidence

ORD record
ord-6923107b9f3f45798b35d04e1b34fa2d
Source dataset
uspto-grants-1988_01
Patent number
US04719036

Reaction notes

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