Butylamine → HCID 70411010, compound

HRID 2413532Notes

Reaction equation

HRID 2413532 reaction equation
[S:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[S:10][CH2:11][CH:12]([C:19]([O:21]CC)=O)[CH2:13][C:14]([O:16]CC)=O.[CH2:24]([NH2:28])[CH2:25][CH2:26][CH3:27]>>[CH2:24]([NH:28][C:14]([CH2:13][CH:12]([C:19]([NH:3][CH2:4][CH2:5][CH2:6][CH3:7])=[O:21])[CH2:11][S:10][C:2]1[S:1][C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=1)=[O:16])[CH2:25][CH2:26][CH3:27]

Participants

3

Reactant 2

HCID 8007ButylamineHCID 20154927HCID 20154927, compound

Product 1

HCID 70411010HCID 70411010, compound

Conditions

Temperature
90 °C

Procedure

18.0 parts of diethyl 3-(benzothiazol-2-ylthio)-propane-1,2-dicarboxylate and 30.0 parts of n-butylamine are stirred for 3 hours at 90° C. Volatile material are removed by heating at 90° C. under a vacuum of 0.1 mm to give N,N'-dibutyl 3-(benzothiazol-2-ylthio)-1,2-propane dicarboxylic acid diamide as a viscous liquid.

Workup

  1. customVolatile material are removed

Sources & evidence

ORD record
ord-1f196038532e4e27b6dd45cc3129cfb1
Source dataset
uspto-grants-1988_01
Patent number
US04719036

Reaction notes

Loading…