HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → Cyclohexanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Solvent | Cyclohexane | HCID 8078 | — |
| Product | Cyclohexanone | HCID 7967 | — |
| Product | Cyclohexene | HCID 8079 | — |
Reaction Steps
In this example, the reaction temperature was set to 240° C., 280° C. and 320° C., respectively. The experimental results were described as follows. When the reaction temperature was 240° C., the selectivity of crude phenol was 100%. However, the increased reaction temperature caused hydrogenation of crude phenol to form cyclohexanone, cyclohexene and even cyclohexane. Thus, in order to produce crude phenol with a high yield, the reaction temperature was set to 240° C. An increase in the reaction temperature caused a low yield of crude phenol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08648218B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-d29682dfa40b471896e4b2ce2e0a2404 |
| Source note | uspto-grants-2014_02 |