HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-2-methyl-1,3-propanediol → 2-(((10-Chloro-1-anthracenyl)methyl)amino)-2-methyl-1,3-propanediol methanesulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-2-methyl-1,3-propanediol | HCID 1531 | — |
| Reactant | 10-Chloroanthracene-1-carbaldehyde | HCID 14391245 | — |
| Reactant | ((10-Chloro9-anthracenyl)methyl)amino-2-methyl-1,3-propanediol methanesulfonate | HCID 86741972 | — |
| Product | 2-(((10-Chloro-1-anthracenyl)methyl)amino)-2-methyl-1,3-propanediol methanesulfonate | HCID 131715425 | — |
Reaction Steps
Using the reductive amination procedure described in 2B, 10-chloroanthracene-1-carbaldehyde (37D) and 2-amino-2-methyl-1,3-propanediol (Aldrich) gave 2-(((10-chloro-1-anthracenyl)methyl)amino)-2-methyl-1,3-propanediol methanesulfonate.9/20H2O mp 230°-231° (dec), (EtOH/Et2O), (C, H, Cl, N, S).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04719049 |
| Source dataset | uspto-grants-1988_01 |
| ORD ID | ord-28523cf520ac43adaf858dbf8d1c8f23 |
| Source note | uspto-grants-1988_01 |