HCID 54139436, compound → HCID 178462165, compound

HRID 2413733Notes

Reaction equation

HRID 2413733 reaction equation
[C:1]1([NH:7][C:8]([NH:10][C@H:11]([C:13]([N:15]2[CH2:29][CH2:28][CH2:27][C@H:16]2[C:17]([N:19]2[CH2:26][CH2:25][CH2:24][C@H:20]2[C:21]([OH:23])=[O:22])=[O:18])=[O:14])[CH3:12])=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[NH2:30][C@H:31]([C:39]([OH:41])=[O:40])[CH2:32][CH2:33][CH2:34][NH:35][C:36](=[NH:38])[NH2:37]>O>[NH2:30][C@H:31]([C:39]([OH:41])=[O:40])[CH2:32][CH2:33][CH2:34][NH:35][C:36](=[NH:37])[NH2:38].[C:1]1([NH:7][C:8]([NH:10][C@H:11]([C:13]([N:15]2[CH2:29][CH2:28][CH2:27][C@H:16]2[C:17]([N:19]2[CH2:26][CH2:25][CH2:24][C@H:20]2[C:21]([OH:23])=[O:22])=[O:18])=[O:14])[CH3:12])=[O:9])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

4

Reactant 2

HCID 54139436HCID 54139436, compoundHCID 178418600HCID 178418600, compound

Product 1

HCID 178462165HCID 178462165, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

N-phenylcarbamoyl-L-alanyl-L-prolyl-L-proline (1.00 g-2.49 m mole) was dissolved in a solution of L-arginine (0.43 g, 2.49 m mole) in water, and the thus obtained solution was freeze-dried to give N-phenylcarbamoyl-L-alanyl-L-prolyl-L-proline L-arginine salt (1.38 g).

Workup

  1. customthe thus obtained solution was freeze-dried

Sources & evidence

ORD record
ord-acad53feb8e8492681e3ca109456039c
Source dataset
uspto-grants-1988_01
Patent number
US04719200

Reaction notes

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