HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → 3-Acetyl-2,2-dimethyl-5-oxo-1-imidazolidineacetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 2,2-Dimethyl-5-oxo-1-imidazolidineacetamide | HCID 20155466 | — |
| Product | 3-Acetyl-2,2-dimethyl-5-oxo-1-imidazolidineacetamide | HCID 20155480 | — |
Reaction Steps
A solution of 2,2 dimethyl-5-oxo-1-imidazolidineacetamide (1.7 g) in acetic anhydride (9 ml) was stirred at 70°-80° C. for 5 minutes. The precipitate was collected and washed with acetone, affording the title compound as a white powder, m.p. 188°-189° C. (ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04719222 |
| Source dataset | uspto-grants-1988_01 |
| ORD ID | ord-6e810c0e2c994e389e5da092147bb860 |
| Source note | uspto-grants-1988_01 |