Isobutyraldehyde → HCID 53959559, compound

HRID 2413749Notes

Reaction equation

[NH2:1][CH2:2][C:3]([NH:5][CH2:6][C:7]([NH:9][CH2:10][C:11]([NH2:13])=[O:12])=[O:8])=[O:4].[CH:14](=O)[CH:15]([CH3:17])[CH3:16]>>[CH:15]([CH:17]1[NH:1][CH2:2][C:3](=[O:4])[N:5]1[CH2:6][C:7]([NH:9][CH2:10][C:11]([NH2:13])=[O:12])=[O:8])([CH3:16])[CH3:14]

Participants

Reactant 2

HCID 6561Isobutyraldehyde

HCID 6427033glycylglycylglycinamide

Product 1

HCID 53959559HCID 53959559, compound

Procedure

The same procedure of example 9, starting from glycylglycylglycinamide and isobutyraldehyde, afforded the title compound as a white hygroscopic solid, m.p. 65°-70° C. Mass spectrum (E.I., 70 eV, 1.5 mA), m/z=199 (M+ --C3H7).

Sources & evidence

ORD record: ord-9d457211ee6b4105a22541253464c9cd
Source dataset: uspto-grants-1988_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04719222

Reaction notes

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