HuagongsheHuagongshe Chemistry Print Report · For research reference only
(+-)(2R*,3R*)-2-Methyl-2-nitro-1,3-butanediol → (+-)(2R*,3S*)-2-amino-2-methyl-1,3-butanediol acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (+-)(2R*,3R*)-2-Methyl-2-nitro-1,3-butanediol | HCID 13375425 | — |
| Reactant | (+-)(2R*,3R*)-2-amino-2-methyl-1,3-butanediol acetate | HCID 86741969 | — |
| Product | (+-)(2R*,3S*)-2-amino-2-methyl-1,3-butanediol acetate | HCID 86741966 | 93% |
Reaction Steps
Using the reduction procedure in 2E, (+-)(2R*,3S*)-2-methyl-2-nitro-1,3-butanediol (2A) gave (+-)(2R*,3S*)-2-amino-2-methyl-1,3-butanediol acetate (93%) (C,H,N) mp 163°-165° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04719236 |
| Source dataset | uspto-grants-1988_01 |
| ORD ID | ord-93a07637961140b1a3ba28cc08db8552 |
| Source note | uspto-grants-1988_01 |