HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2413829Generated: November 1, 2026
Sodium Iodide → Phosphinic acid, P-phenyl-P-(2,4,6-trimethylbenzoyl)-, sodium salt (1:1)
https://huagongshe.com/reaction/2413829
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | Methyl phenyl(2,4,6-trimethylbenzoyl)phosphinate | HCID 20501383 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | Phosphinic acid, P-phenyl-P-(2,4,6-trimethylbenzoyl)-, sodium salt (1:1) | HCID 23690966 | — |
Reaction Steps
60.5 parts by weight of methyl 2,4,6-trimethylbenzoylphenylphosphinate (as described in U.S. Pat. No. 4,265,723) and 33 parts by weight of sodium iodide were dissolved in 560 parts by volume of methyl ethyl ketone, and the solution was stirred for 2.5 hours at 55° C. The resulting precipitate was filtered off, washed with methyl ethyl ketone and dried, the desired product being obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04719297 |
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| Source dataset | uspto-grants-1988_01 |
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| ORD ID | ord-a1a7ab26b1ce44cf9d62448b84b59e81 |
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| Source note | uspto-grants-1988_01 |
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