HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphinic acid, P-phenyl-P-(2,4,6-trimethylbenzoyl)-, sodium salt (1:1) → Phenyl(2,4,6-trimethylbenzoyl)phosphinate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphinic acid, P-phenyl-P-(2,4,6-trimethylbenzoyl)-, sodium salt (1:1) | HCID 23690966 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | Phenyl(2,4,6-trimethylbenzoyl)phosphinate | HCID 18674595 | — |
Reaction Steps
46.5 parts by weight of the sodium salt of Example 1 were dissolved in 300 parts by weight of water, and 150 parts by volume of 1N sulfuric acid were added. The resulting precipitate was filtered off under suction, washed with water and dried, and 38.9 parts by weight of product were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04719297 |
| Source dataset | uspto-grants-1988_01 |
| ORD ID | ord-2fa8484411324ff68d11f97931f1101c |
| Source note | uspto-grants-1988_01 |