Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Chlorohydroxy benzophenone | HCID 6799 | — |
| Reactant | 3-Pyridinecarbonyl chloride, hydrochloride (1:1) | HCID 88438 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 70408025 | HCID 70408025 | — |
Reaction Steps
15 g (64.5 mmol) of p-chlorobenzoylphenol and 12 g (68 mmol) of nicotinic acid chloride hydrochloride was mixed with 200 ml dry pyridine and stirred for 24 hours at 40° C. After cooling 200 ml water were added and the precipitated product washed twice with 80 ml of water and recrystallized from methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | USRE032581 |
|---|
| Source dataset | uspto-grants-1988_01 |
|---|
| ORD ID | ord-4c70fe3ffda3441e8ef267923006c6c7 |
|---|
| Source note | uspto-grants-1988_01 |
|---|
