HRID2413872
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
产物
AUXILIARIES
试剂、催化剂与溶剂
CONDITIONS
反应条件
- 温度
- 95 °C
PROCEDURE
实验过程
A mixture of 69.6 grams (0.589 mole) of ammonium metavanadate, 342.0 grams (2.356 moles) of 2-ethylhexanoate (acid number 387) and 130 grams of mineral spirits was heated to 95° C. and held for 1 hour without reaction occurring. The temperature was gradually increased to 195° C. in 3.5 hours while the water of reaction was removed. The reaction product solidified at room temperature.
WORKUP
后处理
- customheld for 1 hour without reaction
- customwas removed
- customsolidified at room temperature