Ammonium metavanadate → HCID 178443853, compound

HRID 2413872Notes

Reaction equation

HRID 2413872 reaction equation
[NH4+].[O-][V:3](=O)=O.[CH2:6]([CH:8]([CH2:12][CH2:13][CH2:14][CH3:15])[C:9]([O-:11])=[O:10])[CH3:7]>O>[CH2:6]([CH:8]([CH2:12][CH2:13][CH2:14][CH3:15])[C:9]([O-:11])=[O:10])[CH3:7].[V+5:3].[CH2:6]([CH:8]([CH2:12][CH2:13][CH2:14][CH3:15])[C:9]([O-:11])=[O:10])[CH3:7].[CH2:6]([CH:8]([CH2:12][CH2:13][CH2:14][CH3:15])[C:9]([O-:11])=[O:10])[CH3:7].[CH2:6]([CH:8]([CH2:12][CH2:13][CH2:14][CH3:15])[C:9]([O-:11])=[O:10])[CH3:7].[CH2:6]([CH:8]([CH2:12][CH2:13][CH2:14][CH3:15])[C:9]([O-:11])=[O:10])[CH3:7]

Participants

4

Reactant 2

HCID 516859Ammonium metavanadateHCID 40723562-Ethylhexanoate

Product 1

HCID 178443853HCID 178443853, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Conditions

Temperature
95 °C

Procedure

A mixture of 69.6 grams (0.589 mole) of ammonium metavanadate, 342.0 grams (2.356 moles) of 2-ethylhexanoate (acid number 387) and 130 grams of mineral spirits was heated to 95° C. and held for 1 hour without reaction occurring. The temperature was gradually increased to 195° C. in 3.5 hours while the water of reaction was removed. The reaction product solidified at room temperature.

Workup

  1. customheld for 1 hour without reaction
  2. customwas removed
  3. customsolidified at room temperature

Sources & evidence

ORD record
ord-3f265e6cfeaa474ea855713dafdd4773
Source dataset
uspto-grants-1988_01
Patent number
US04720352

Reaction notes

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