HRID2413872

反应详情

EQUATION

反应方程式

HRID 2413872 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
95 °C

PROCEDURE

实验过程

A mixture of 69.6 grams (0.589 mole) of ammonium metavanadate, 342.0 grams (2.356 moles) of 2-ethylhexanoate (acid number 387) and 130 grams of mineral spirits was heated to 95° C. and held for 1 hour without reaction occurring. The temperature was gradually increased to 195° C. in 3.5 hours while the water of reaction was removed. The reaction product solidified at room temperature.

WORKUP

后处理

  1. customheld for 1 hour without reaction
  2. customwas removed
  3. customsolidified at room temperature