HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 2-Methyl-3-(trichlorogermyl)butanoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 13249025 | HCID 13249025 | — |
| Product | 2-Methyl-3-(trichlorogermyl)butanoyl chloride | HCID 13249038 | 90.4% |
Reaction Steps
28.0 g (0.1 mol) of 2-methyl-3-(trichlorogermyl)butanoic acid was treated with 100 ml of thionyl chloride. The reaction mixture was distilled under a reduced pressure to obtain 27.0 g of 2-methyl-3-(trichlorogermyl)butanoyl chloride as a pale yellow portion having a boiling point of 99° to 100° C./6 mmHg (yield: 90.4%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04720564 |
| Source dataset | uspto-grants-1988_01 |
| ORD ID | ord-7773676fdbee4db6afa201097edbceef |
| Source note | uspto-grants-1988_01 |