Oxygen → Methacrylic Acid

Participants

Reaction Steps

A vaporous mixture of isobutyric acid and oxygen (as air) in a molar ratio of 1:1:5 was conducted at 340° C. over 169.9 g (130 ml) of the orange colored bead catalyst in a recirculating reactor with a loading of the pure catalyst mass of 2.364 (10-4) mole of isobutyric acid per gram of catalytic mass and per minute. Under these conditions, an isobutyric acid conversion of 70.2% and a selectivity of methacrylic acid of 76% were obtained. The space-time yield of methacrylic acid was 287 grams/liter/hour.

Provenance & Evidence