HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N'-Diisopropyl-1,3-propanediamine → HCID 14096737, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N'-Diisopropyl-1,3-propanediamine | HCID 144018 | — |
| Reactant | 3,4-Dimethoxybenzenesulfonyl chloride | HCID 2734183 | — |
| Product | HCID 14096737 | HCID 14096737 | — |
Reaction Steps
3,4 Dimethoxybenzenesulfonyl chloride was reacted with N,N'-diisopropylpropane-1,3-diamine by procedures following those given in Example 1 and chromatographed on Dry-column alumina with 10% methanol/ethyl acetate to provide the title compound. Treatment of this material with isopropanol/HCl gave the hydrochloride salt, m.p. 132°-135° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04720580 |
| Source dataset | uspto-grants-1988_01 |
| ORD ID | ord-dfba550e3a03420597ed1ac7680b542f |
| Source note | uspto-grants-1988_01 |